Triethylamine → HCID 56636674, compound

HRID 27874

Reaction equation

[C:1]([OH:20])(=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12]CCCC(C)C.C(N([CH2:26][CH3:27])CC)C>>[CH2:1]([O:20][CH:2]([CH2:3][CH2:4][CH2:5][CH2:6][CH2:26][CH3:27])[CH3:1])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

Reactant 2

HCID 8471Triethylamine

HCID 2185916-Methylheptadecanoic Acid

Product 1

HCID 56636674HCID 56636674, compoundYield 5,000%

Conditions

Temperature: 130 °C

Procedure

To 32 g (0.1 mole) of isostearic acid there is added 0.3 ml (0.002 mole) of triethylamine. The resulting mixture is heated to 130° C. under a nitrogen atmosphere and there are slowly added thereto 40 g (0.1 mole) of 2-octyl dodecyl ether of glycidyl obtained according to the above method. After heating for 3 hours and 15 minutes at 130° C., the amount of the reaction determined by acid index is 93%.

Workup

additionthere are slowly added

Sources & evidence

ORD record: ord-2dc269c23b514a9789547f511597a9fb
Source dataset: uspto-grants-1980_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04224311

Linked notes

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