HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Phenylhydroxylamine → 1-(4-chlorophenyl)-N-phenylmethanimine oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Phenylhydroxylamine | HCID 7518 | — |
| Reactant | N-(p-Chlorobenzylidene)-2-methyl-4-chloroaniline | HCID 13017552 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 1-(4-chlorophenyl)-N-phenylmethanimine oxide | HCID 254504 | — |
Reaction Steps
N-phenylhydroxylamine (0.052 mole) was dissolved in ether (20 cc). This solution was treated with N-(p-chlorobenzylidene)-2-methyl-4-chloroaniline (13.8 g.) dissolved in ether (50 cc). After 15 min., white crystals had begun to form. Filtration and washing with ether gave α-p-chlorophenyl-N-phenylnitrone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04224340 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-0e12529043b64c969cf8dc80bad688c5 |
| Source note | uspto-grants-1980_09 |