HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylglyoxal → N-(3-(4-Methylphenyl)propyl)-2-hydroxy-2-phenylethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylglyoxal | HCID 14090 | — |
| Reactant | 3-(4-Methylphenyl)propan-1-amine | HCID 12564270 | — |
| Product | N-(3-(4-Methylphenyl)propyl)-2-hydroxy-2-phenylethanamine | HCID 20212420 | — |
Reaction Steps
The title compound was prepared in the manner described in Example 9 using phenylglyoxal and 3-(4-Methylphenyl)propanamine. Recrystallization of the chromatographed material from benzene-hexane gave the title compound m.p. 114-116. τ(CDCL3) 8.15 (2H, m), 7.7 (3H, s), 6.9-7.5 (6H, m+2H, disappears with D2O), 5.3 (1H, m), 2.9 (4H, s), 2.7 (5H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04588749 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-ee42504e3d654a9b9c7dea16de494dc3 |
| Source note | uspto-grants-1986_05 |