Thioglycolic Acid → Cyclooctyl mercaptoacetate

HRID 280498

Reaction equation

HRID 280498 reaction equation
[CH:1]1([OH:9])[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[SH:10][CH2:11][C:12](O)=[O:13].C1(C)C=CC(S(O)(=O)=O)=CC=1>>[SH:10][CH2:11][C:12]([O:9][CH:1]1[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1)=[O:13]

Participants

4

Reactant 3

HCID 1133Thioglycolic AcidHCID 6101p-Toluenesulfonic acidHCID 12766Cyclooctanol

Product 1

HCID 20212358Cyclooctyl mercaptoacetate

Procedure

Into a 100 ml reaction flask equipped with stirrer, thermometer, reflux condenser and heating mantle are placed 32 grams of cyclooctanol; 9.2 grams of mercaptoacetic acid and 0.5 grams paratoluene sulfonic acid.

Workup

  1. customInto a 100 ml reaction flask
  2. customequipped with stirrer
  3. temperaturethermometer, reflux condenser
  4. temperatureheating mantle

Sources & evidence

ORD record
ord-e02bfdc43ff3476392826e50b8b1bd94
Source dataset
uspto-grants-1986_05
Patent number
US04590082

Linked notes

Loading…