p-Toluenesulfonic acid → (4'-t-BUTYLCYCLOHEXYL)-3-MERCAPTO-PROPIONATE

HRID 280500

Reaction equation

HRID 280500 reaction equation
[C:1]([CH:5]1[CH2:10][CH2:9][CH:8]([OH:11])[CH2:7][CH2:6]1)([CH3:4])([CH3:3])[CH3:2].C1(C)C=CC(S(O)(=O)=O)=CC=1.[SH:23][CH2:24][CH2:25][C:26](O)=[O:27]>>[C:1]([CH:5]1[CH2:6][CH2:7][CH:8]([O:11][C:26](=[O:27])[CH2:25][CH2:24][SH:23])[CH2:9][CH2:10]1)([CH3:4])([CH3:2])[CH3:3]

Participants

4

Reactant 3

HCID 6101p-Toluenesulfonic acidHCID 65143-Mercaptopropionic AcidHCID 73914-tert-Butylcyclohexanol

Product 1

HCID 20212366(4'-t-BUTYLCYCLOHEXYL)-3-MERCAPTO-PROPIONATE

Procedure

Into a 100 ml reaction flask equipped with reflux condenser, hot plate, spin bar and thermometer are placed 15.5 grams of 4-t-butylcyclohexanol; 0.5 grams paratoluene sulfonic acid and 15.5 grams of 3-mercapto-propionic acid.

Workup

  1. customInto a 100 ml reaction flask
  2. customequipped
  3. temperaturewith reflux condenser

Sources & evidence

ORD record
ord-c6cd72a204b9469bb983cae0f67fefb9
Source dataset
uspto-grants-1986_05
Patent number
US04590082

Linked notes

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