2-Pentanone → 1-(2',6'-Diethylphenyl)-4-methylamino-1,2-dihydro-1,3,5-triazin-one

HRID 28054

Reaction equation

HRID 28054 reaction equation
[CH2:1]([C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([CH2:9][CH3:10])[C:4]=1[NH:11][C:12]([NH:14][C:15](=[NH:18])[NH:16][CH3:17])=[O:13])[CH3:2].[CH3:19]C(=O)CCC>CCCCCC>[CH2:9]([C:5]1[CH:6]=[CH:7][CH:8]=[C:3]([CH2:1][CH3:2])[C:4]=1[N:11]1[CH:17]=[N:16][C:15]([NH:18][CH3:19])=[N:14][C:12]1=[O:13])[CH3:10]

Participants

4

Reactant 2

HCID 78952-PentanoneHCID 178436233HCID 178436233, compound

Product 1

HCID 130393601-(2',6'-Diethylphenyl)-4-methylamino-1,2-dihydro-1,3,5-triazin-one

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

The same procedure is followed as in Example 4 above using 1-(2',6'-diethylphenyl)-3-methylamidinourea as the starting material and using as the recrystallization medium a mixed solvent of pentanone and hexane (30:10).

Sources & evidence

ORD record
ord-37e72e711f704f7884b0216a6eb05d0d
Source dataset
uspto-grants-1980_09
Patent number
US04225315

Linked notes

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