3-Anilinopropionitrile → HCID 70474354, compound

HRID 280706

Reaction equation

HRID 280706 reaction equation
[CH:1]1[CH:6]=[C:5]2[C:7]([CH:10]=O)=[CH:8][S:9][C:4]2=[CH:3][CH:2]=1.[NH:12]([CH2:19][CH2:20][C:21]#[N:22])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>O>[NH:12]([CH:19]=[C:20]([CH2:10][C:7]1[C:5]2[CH:6]=[CH:1][CH:2]=[CH:3][C:4]=2[S:9][CH:8]=1)[C:21]#[N:22])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

4

Reactant 2

HCID 141003-AnilinopropionitrileHCID 2273281-Benzothiophene-3-carbaldehyde

Product 1

HCID 70474354HCID 70474354, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The title compound was prepared from thianaphthene-3-carboxaldehyde (W. J. King and F. F. Nord, J. Org. Chem. 1948, 13, 635) and 3-anilinopropionitrile by the procedure of Example 4A (29%); mp 168°-170° dec. Anal. Calcd for C18H14N2S: 0.1 H2O: C, 73.99; H, 4.90; N, 9.59; S, 10.97. Found: C, 74.03; H, 5.21; N, 9.59; S, 11.01.

Sources & evidence

ORD record
ord-55d7daeaea624124a8432373072b9aee
Source dataset
uspto-grants-1986_05
Patent number
US04590271

Linked notes

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