Phosphorus oxychloride → HCID 86612216, compound

HRID 29957Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:18]3[C:13](=[CH:14][C:15]([CH3:19])=[CH:16][CH:17]=3)[C:12](=O)[NH:11][N:10]=2)=[CH:5][CH:4]=1.P(Cl)(Cl)([Cl:23])=O>>[Cl:23][C:12]1[C:13]2[C:18](=[CH:17][CH:16]=[C:15]([CH3:19])[CH:14]=2)[C:9]([C:6]2[CH:7]=[CH:8][C:3]([O:2][CH3:1])=[CH:4][CH:5]=2)=[N:10][N:11]=1

Participants

Reactant 2

HCID 24813Phosphorus oxychloride

HCID 692108744-(4-methoxyphenyl)-7-methyl-2H-phthalazin-1-one

Product 1

HCID 86612216HCID 86612216, compound

Procedure

This compound is obtained according to the procedure described in 1.3. by reacting 4-(4-methoxyphenyl)-7-methyl-2H-phthalazin-1-one with phosphoryl chloride.

Workup

customThis compound is obtained

Sources & evidence

ORD record: ord-d25ae0751c414fe9bf8f743eb22bbed7
Source dataset: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07423030B2

Reaction notes

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