Hydrazine hydrate (1:1) → 7-methoxy-4-methyl-2H-phthalazin-1-one

HRID 30017

Reaction equation

HRID 30017 reaction equation
[C:1]([C:4]1[CH:12]=[CH:11][C:10]([O:13][CH3:14])=[CH:9][C:5]=1[C:6](O)=[O:7])(=O)[CH3:2].O.[NH2:16][NH2:17]>>[CH3:14][O:13][C:10]1[CH:9]=[C:5]2[C:4]([C:1]([CH3:2])=[N:16][NH:17][C:6]2=[O:7])=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 201632832-Acetyl-5-methoxybenzoic acid

Product 1

HCID 576916797-methoxy-4-methyl-2H-phthalazin-1-one

Procedure

This compound is obtained according to the procedure described in 1.2. by reacting unpurified 2-acetyl-5-methoxybenzoic acid with hydrazine hydrate.

Workup

  1. customThis compound is obtained

Sources & evidence

ORD record
ord-c6a4856f01e34ed292e04c7d725ac6d0
Source dataset
uspto-grants-2008_09
Patent number
US07423030B2

Linked notes

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