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Methanol → HCID 20462167, compound

HRID 326111
Notes
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Reaction equation

HRID 326111 reaction equation
Br[CH2:2][C:3](OC)([CH3:6])[CH2:4][OH:5].[Na].[CH2:10]([SH:28])[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27].CO>C(O)C>[CH2:6]=[C:3]([CH2:2][S:28][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27])[CH2:4][OH:5]
ParticipantsProcedureSources & evidenceReaction notes

Participants

6

Reactant 4

HCID 887MethanolHCID 179051-OctadecanethiolHCID 5360545SodiumHCID 204623593-Bromo-2-methoxy-2-methylpropan-1-ol

Product 1

HCID 20462167HCID 20462167, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

3-Bromo-2-methoxy-2-methylpropan-1-ol is reacted with the sodium salt of octadecanethiol in ethanol. The 2-methylene-3-octadecylthiopropan-1-ol (wax-like substance) is thereby obtained with the splitting off of methanol.

Sources & evidence

ORD record
ord-e9cf853b0ce14ee48f7cd2cd76278d59
Source dataset
uspto-grants-1984_04
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US04444766

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes