Silver → Silver neo-decanoate cumene

HRID 330464

Reaction equation

HRID 330464 reaction equation
[C:1]([OH:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([CH3:10])([CH3:9])[CH3:8].[Ag:13]=O.[Ag]>C1(C(C)C)C=CC=CC=1>[C:1]([O-:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([CH3:8])([CH3:9])[CH3:10].[Ag+:13].[C:6]1([CH:7]([CH3:9])[CH3:10])[CH:1]=[CH:2][CH:3]=[CH:4][CH:5]=1

Participants

5

Reactant 3

HCID 23954SilverHCID 62838Versatic 10HCID 92152Silver(II) oxide

Product 1

HCID 86743715Silver neo-decanoate cumene

Reagents, catalysts & solvents 1

HCID 7406CumeneSolvent3×

Procedure

A silver neo-decanoate/cumene solution is prepared from 539.00 gm of neo-decanoic acid (obtained from Exxon Chemical Co.), 350.00 gm of cumene (obtained from Aldrich Chemical Co.), and an excessive amount of silver oxide (392.21 gm) in a similar manner to that described in Example 1 of U.S. Pat. No. 4,663,303. A 496.42 gm sample of this solution is diluted with 19.35 gm of cumene to yield a solution having a weight ratio of silver salt/cumene of 2.2/1.0.

Workup

  1. customto yield a solution

Sources & evidence

ORD record
ord-d2c0f7c7c4154c5f8845b0f551d76916
Source dataset
uspto-grants-1990_01
Patent number
US04897376

Linked notes

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