Oxalyl chloride → Oleoyl chloride

HRID 344759

Reaction equation

HRID 344759 reaction equation
[C:1]([OH:20])(=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].C(Cl)(=O)C([Cl:24])=O>CCCCCC>[C:1]([Cl:24])(=[O:20])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

4

Reactant 2

HCID 65578Oxalyl chlorideHCID 445639Oleic Acid

Product 1

HCID 5364783Oleoyl chloride

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

A 1.0 g portion of oleic acid was dissolved in 10 ml of hexane. A 2.0 ml portion of oxalyl chloride was added and this mixture was stirred under dry conditions for 1.5 hours, then evaporated in vacuo, giving the desired compound as a colorless oil.

Workup

  1. customevaporated in vacuo

Sources & evidence

ORD record
ord-cb048427a94349fe96c65f45efcdb2bf
Source dataset
uspto-grants-1991_10
Patent number
US05053426

Linked notes

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