3-Amino-1,2-propanediol → N-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoyl)-3-amino-1,2-propanediol

HRID 34571

Reaction equation

HRID 34571 reaction equation
[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])=[CH:3][C:4]([OH:6])=O.[NH2:23][CH2:24][CH:25]([OH:28])[CH2:26][OH:27]>>[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])=[CH:3][C:4]([NH:23][CH2:24][CH:25]([OH:28])[CH2:26][OH:27])=[O:6]

Participants

3

Reactant 2

HCID 735613-Amino-1,2-propanediolHCID 1285703,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenic acid

Product 1

HCID 54513141N-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoyl)-3-amino-1,2-propanediolYield 86%

Procedure

The same procedure as in Example 1 was repeated except that 6.1 g of 3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid and 1.9 g of 3-amino-1,2-propanediol were used as the starting materials. 6.5 g (86%) of the title compound was obtained as a white wax.

Sources & evidence

ORD record
ord-17d07784cbee4d7cba095840330a8758
Source dataset
uspto-grants-1988_08
Patent number
US04762829

Linked notes

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