2-Methylheptanoic acid → 2-Methylheptanoyl chloride

HRID 35716

Reaction equation

[CH3:1][CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])[C:3](O)=[O:4].C(Cl)(=O)C([Cl:14])=O>>[CH3:1][CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])[C:3]([Cl:14])=[O:4]

Participants

Reactant 2

HCID 144752-Methylheptanoic acid

HCID 65578Oxalyl chloride

Product 1

HCID 142345192-Methylheptanoyl chloride

Procedure

Employing 5 g. of 2-methylheptanoic acid and 7.6 ml. of oxalyl chloride and using the procedure of Preparation A2, 3.3 g. of the desired product was obtained, b.p. 32°-34 ° C./0.6 torr.

Sources & evidence

ORD record: ord-1fc6288efb9444c8a053a08633c41fe3
Source dataset: uspto-grants-1988_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04767743

Linked notes

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