Isopropanol → Isopropyl Trichloroacrylate
Reaction equation
[CH:1]([OH:4])([CH3:3])[CH3:2].[Cl:5][C:6](=[C:10]([Cl:12])[Cl:11])[C:7](Cl)=[O:8]>C(Cl)Cl>[Cl:11][C:10]([Cl:12])=[C:6]([Cl:5])[C:7]([O:4][CH:1]([CH3:3])[CH3:2])=[O:8]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of 6.5 gms (0.108 moles) isopropyl alcohol, 20 gms (0.013 moles) trichloro acryloyl chloride and 100 ml methylene chloride was stirred for 72 hours. The solvent was stripped and the product was used in subsequent reactions without further purification.
Workup
- customthe product was used in subsequent reactions without further purification
Sources & evidence
- ORD record
- ord-4cc9112742054be59544a64647003c56
- Source dataset
- uspto-grants-1984_08
- Patent number
- US04465690
Reaction notes
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