1,1-Dimethylhydrazine → HCID 54468337, compound
Reaction equation
[CH3:1][O:2][C:3](=[CH2:6])[CH:4]=O.[CH3:7][N:8]([CH3:10])[NH2:9]>CCOCC>[CH3:1][O:2][C:3]([CH:4]=[N:9][N:8]([CH3:10])[CH3:7])=[CH2:6]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
6.4 g of 2-methoxyacrolein are stirred for 1 hour at 30°-35° C. with 4.4 g of N,N-dimethylhydrazine in 50 ml of ether, dried at 20° C. with Na2SO4 and then the solvent is removed. Distillation at 74°-76° C./13 mbar gives 6.2 g of pure 2-methoxy-4-dimethylamino-4-azabutadiene.
Workup
- dry with materialdried at 20° C. with Na2SO4
- customthe solvent is removed
- distillationDistillation at 74°-76° C./13 mbar
Sources & evidence
- ORD record
- ord-3e8bd73790e24c7db9db22dd813cbd3e
- Source dataset
- uspto-grants-1991_03
- Patent number
- US04999426
Reaction notes
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