Potassium Carbonate → HCID 178472280, compound

HRID 36451Notes

Reaction equation

HRID 36451 reaction equation
[CH2:1]([O:3][CH:4]([PH:8](=[O:12])OCC)[O:5][CH2:6][CH3:7])[CH3:2].[CH2:13]([Mg]Cl)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.C(=O)([O-])[O-].[K+].[K+]>C(OCC)C.O>[CH2:13]([PH:8](=[O:12])[CH:4]([O:3][CH2:1][CH3:2])[O:5][CH2:6][CH3:7])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

6

Reactant 3

HCID 11430Potassium CarbonateHCID 178418336HCID 178418336, compoundHCID 178472284HCID 178472284, compound

Product 1

HCID 178472280HCID 178472280, compound

Reagents, catalysts & solvents 2

HCID 962WaterSolventHCID 3283Diethyl EtherSolvent

Procedure

By a procedure analogous to that of Example 1, but using 1.96 g of ethyl diethoxymethylphosphinate and 20 ml of a molar solution of benzylmagnesium chloride in diethyl ether and adding 4.14 g of potassium carbonate in 5 ml of water to precipitate inorganic salts, benzyl(diethoxymethyl)phosphine oxide is obtained as a colourless oil.

Workup

  1. customto precipitate inorganic salts

Sources & evidence

ORD record
ord-5d1b7b05088e43aab4f8c5301d4e457c
Source dataset
uspto-grants-1995_05
Patent number
US05414133

Reaction notes

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