Hydrogen Peroxide → HCID 178444799, compound

HRID 36540

Reaction equation

HRID 36540 reaction equation
[CH2:1]([CH:5]([CH2:9][NH:10][CH2:11][CH2:12][C:13]([OH:15])=[O:14])[C:6]([OH:8])=[O:7])[CH2:2][CH2:3][CH3:4].C(N(CC(O)=O)CC(O)=O)CN(CC(O)=O)CC(O)=[O:21].OO>O>[CH2:1]([CH:5]([CH2:9][NH:10][CH2:11][CH2:12][C:13]([OH:15])=[O:14])[C:6]([OH:8])=[O+:7][O-:21])[CH2:2][CH2:3][CH3:4]

Participants

5

Reactant 3

HCID 784Hydrogen PeroxideHCID 6049Ethylenediaminetetraacetic AcidHCID 131718997Butyl imino dipropionic acid

Product 1

HCID 178444799HCID 178444799, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
50 °C

Procedure

100 g butyl imino dipropionic acid (0.46 mol) from example 7a was dissolved in 100 g H2O, whereupon 0.10 g EDTA was added and the temperature was increased to 50° C. After 30 minutes 3.2 g (0.475 mol) 50% hydrogen peroxide was added by drops during 20 minutes and the mixture reacted for 2 hours at 75° C. under a reflux cooler. Then the water was evaporated at 40° C. until a slightly yellow-brown oil formed.

Workup

  1. additionwas added
  2. customthe mixture reacted for 2 hours at 75° C. under a reflux cooler
  3. customThen the water was evaporated at 40° C. until a slightly yellow-brown oil
  4. customformed

Sources & evidence

ORD record
ord-21e0230d66d34335bfad3ff73829e671
Source dataset
uspto-grants-1995_05
Patent number
US05415668

Linked notes

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