N-Butylaniline → 7-Hydroxy-2-(N-butylanilinocarbonyl)-I,4-benzodioxin

HRID 37176

Reaction equation

HRID 37176 reaction equation
[CH2:1]([NH:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH3:4].[OH:12][C:13]1[CH:14]=[CH:15][C:16]2[O:21][CH:20]=[C:19]([C:22](O)=[O:23])[O:18][C:17]=2[CH:25]=1>>[OH:12][C:13]1[CH:14]=[CH:15][C:16]2[O:21][CH:20]=[C:19]([C:22]([N:5]([CH2:1][CH2:2][CH2:3][CH3:4])[C:6]3[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=3)=[O:23])[O:18][C:17]=2[CH:25]=1

Participants

3

Reactant 2

HCID 14310N-ButylanilineHCID 109323117-Hydroxy-1,4-benzodioxin-2-carboxylic acid

Product 1

HCID 108710697-Hydroxy-2-(N-butylanilinocarbonyl)-I,4-benzodioxinYield 78%

Procedure

That compound is obtained in a yield of 78% starting from N-butylaniline and 7-hydroxy-1,4-benzodioxin-2-carboxylic acid.

Workup

  1. customThat compound is obtained in a yield of 78%

Sources & evidence

ORD record
ord-99821b20530c4a8aa920baea154b5d6a
Source dataset
uspto-grants-1995_05
Patent number
US05420132

Linked notes

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