Methylcarbamyl fluoride → N-Methyl-N-(n-Octylthiosulfenyl)Carbamoyl Fluoride
Reaction equation
[CH2:1]([S:9][S:10]Cl)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH3:12][NH:13][C:14]([F:16])=[O:15]>C(N(CC)CC)C>[CH3:12][N:13]([S:10][S:9][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[C:14]([F:16])=[O:15]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Prepared as above by adding 25.2 g triethylamine to a solution of 48.0 g. n-octylthiosulfenylchloride and 19.26 g N-methylcarbamoyl fluoride. b.p. 110°-118° C/0.2 Torr. ND21 1.4900.
Workup
- customPrepared as above
Sources & evidence
- ORD record
- ord-44a631b71869410598a19aae6c2cc912
- Source dataset
- uspto-grants-1978_05
- Patent number
- US04091016
Reaction notes
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