Bisphenol A diglycidyl ether → Bisphenol A
Reaction equation
C([O:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]([C:15]2[CH:20]=[CH:19][C:18]([O:21]CC3OC3)=[CH:17][CH:16]=2)([CH3:14])[CH3:13])=[CH:8][CH:7]=1)C1OC1.C(O)(=O)C=C.C(C1CC(=O)OC1=O)=CCCCCCC>>[OH:5][C:6]1[CH:7]=[CH:8][C:9]([C:12]([C:15]2[CH:16]=[CH:17][C:18]([OH:21])=[CH:19][CH:20]=2)([CH3:14])[CH3:13])=[CH:10][CH:11]=1Participants
4
Procedure
10.54 g of bisphenol A diglycidyl ether was heated to 70 C. under stirring and then 4.46 g acrylic acid was added slowly under nitrogen atmosphere. After maintaining the reaction at 70 C. for 2 hours, 13.0 g of 2-octen-1-ylsuccinic anhydride was added and then the temperature was raised to 80 C. under mechanical stirring. The reactants are stirred at 80 C. for 2-3 hours to complete the reaction.
Workup
- temperatureAfter maintaining
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