Ethylene Glycol → HCID 55276487, compound

Reaction equation

C(O)C[OH:3].C1(C)C=C[C:8]([S:11](O)(=O)=O)=[CH:7]C=1.[C:16]1([CH3:22])[CH:21]=[CH:20][CH:19]=C[CH:17]=1.[OH2:23]>>[C:8]([O:23][CH:21]([CH2:20][CH3:19])[CH:16]([CH3:22])[CH:17]=[O:3])(=[S:11])[CH3:7]

Participants

Reactant 4

HCID 174Ethylene Glycol

HCID 962Water

HCID 1140Toluene

HCID 6101p-Toluenesulfonic acid

Product 1

HCID 55276487HCID 55276487, compound

Procedure

10 g (57 mmol) of the compound as prepared above are boiled with 7.01 g (114 mmol) of ethylene glycol, 150 mg of p-toluenesulfonic acid and 300 ml of toluene for 3 hours with reflux at the water separator.

Sources & evidence

ORD record: ord-a448b91fe08040cba325750a23007511
Source dataset: uspto-grants-2001_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06303173B1

Reaction notes

Loading…