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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 399079Generated: October 26, 2026

4-Methylthiobenzyltriphenylphosphonium chloride → (E)-1-(Methylthio)-4-[2-(4-methylthiophenyl)ethenyl]benzene

https://huagongshe.com/reaction/399079

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Methylthiobenzyltriphenylphosphonium chlorideHCID 18969794—
CatalystBenzyltriphenylphosphonium chlorideHCID 70671—
Product(E)-1-(Methylthio)-4-[2-(4-methylthiophenyl)ethenyl]benzeneHCID 12652959—

Reaction Steps

Following the procedure as describe in method 1, but sustituting 4-methylthiobenzyltriphenylphosphonium chloride for benzyltriphenylphosphonium chloride, the desired residue was purified by flash chromatography (silica gel; hexane/EtOAc (90:10)) and recrystallisation from hexane.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05817700
Source datasetuspto-grants-1998_10
ORD IDord-92dd2f6185b44d6eb92558a7134d09c5
Source noteuspto-grants-1998_10