9-Decenoic acid → Octadec-9-enyl dec-9-enoate

HRID 400346

Reaction equation

HRID 400346 reaction equation
[CH2:1]([OH:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[C:20](O)(=[O:30])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH:28]=[CH2:29]>C(OCC)(=O)C.CCCCCC>[C:20]([O:19][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]=[CH:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])(=[O:30])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH:28]=[CH2:29]

Participants

4

Reactant 2

HCID 617439-Decenoic acidHCID 5284499Oleyl Alcohol

Product 1

HCID 86669121Octadec-9-enyl dec-9-enoateYield 96%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Compound E was prepared from Oleyl alcohol and 9-decenoic acid following the general procedure previously discussed and shown in FIG. 10. Pure compound E was a colorless oil obtained by column chromatography with Ethyl acetate/Hexane=1:40.

Sources & evidence

ORD record
ord-768740c8253947a09478f0ca8eb919de
Source dataset
uspto-grants-2014_06
Patent number
US08741822B2

Linked notes

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