1-Bromopentane → HCID 21281115, compound

Reaction equation

[C:1]1([N:7]2[CH:11]=[CH:10][C:9]([CH:12]=[O:13])=[CH:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Mg].Br[CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]>>[OH:13][CH:12]([C:9]1[CH:10]=[CH:11][N:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH:8]=1)[CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]

Participants

Reactant 3

HCID 80571-Bromopentane

HCID 5462224Magnesium

HCID 10920962HCID 10920962, compound

Product 1

HCID 21281115HCID 21281115, compoundYield 95.9%

Procedure

This compound was synthesized according to the procedure described in Example 3. Thus, starting from 2.2 g of 1-phenylpyrrole-3-aldehyde, 1.2 g of magnesium and 3.8 g of 1-bromopentane, 3 g of pure product was obtained as an oil.

Workup

customThis compound was synthesized

Sources & evidence

ORD record: ord-ea57e34fbd954bf2b4aca5f179b71ba8
Source dataset: uspto-grants-1988_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04792568

Reaction notes

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