Diethylmethylamine → Methanesulfonic acid, 1,1,1-trifluoro-, compd. with N-ethyl-N-methylethanamine (1:1)

HRID 41837Notes

Reaction equation

HRID 41837 reaction equation
[CH2:1]([N:3]([CH2:5][CH3:6])[CH3:4])[CH3:2].[F:7][C:8]([F:14])([F:13])[S:9]([OH:12])(=[O:11])=[O:10]>>[F:7][C:8]([F:14])([F:13])[S:9]([O-:12])(=[O:11])=[O:10].[CH2:1]([NH+:3]([CH2:5][CH3:6])[CH3:4])[CH3:2]

Participants

3

Reactant 2

HCID 12022Diethylmethylamine2×HCID 62406Trifluoromethanesulfonic acid2×

Product 1

HCID 86620365Methanesulfonic acid, 1,1,1-trifluoro-, compd. with N-ethyl-N-methylethanamine (1:1)

Procedure

Equimolar amounts of diethylmethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed diethylmethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

Workup

  1. temperaturewhile being cooled by liquid nitrogen
  2. customthus obtaining a target ionic conductor

Sources & evidence

ORD record
ord-424cd18c450e45828a8725a8621ee747
Source dataset
uspto-grants-2013_09
Patent number
US08535849B2

Reaction notes

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