Trifluoromethanesulfonic acid → Ethylpiperidinium Trifluoromethanesulfonate

Reaction equation

[CH2:1]([NH+:3]1[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1)[CH3:2].[F:9][C:10]([F:16])([F:15])[S:11]([OH:14])(=[O:13])=[O:12]>>[F:9][C:10]([F:16])([F:15])[S:11]([O-:14])(=[O:13])=[O:12].[CH2:1]([NH+:3]1[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1)[CH3:2]

Participants

Reactant 2

HCID 62406Trifluoromethanesulfonic acid2×

HCID 6992606HCID 6992606, compound2×

Product 1

HCID 23134843Ethylpiperidinium Trifluoromethanesulfonate

Procedure

Equimolar amounts of ethylpiperidinium and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed ethylpiperidinium and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

Workup

temperaturewhile being cooled by liquid nitrogen
customthus obtaining a target ionic conductor

Sources & evidence

ORD record: ord-85528ab2c6dd45e5a5e1a95ecacf1a20
Source dataset: uspto-grants-2013_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08535849B2

Reaction notes

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