Reaction equation
[CH3:1][N:2]([CH3:5])[CH2:3][CH3:4].[F:6][C:7]([F:13])([F:12])[S:8]([OH:11])(=[O:10])=[O:9]>>[F:6][C:7]([F:13])([F:12])[S:8]([O-:11])(=[O:10])=[O:9].[CH3:1][NH+:2]([CH3:5])[CH2:3][CH3:4]Participants
3
Procedure
Equimolar amounts of dimethylethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed dimethylethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.
Workup
- temperaturewhile being cooled by liquid nitrogen
- customthus obtaining a target ionic conductor
Sources & evidence
- ORD record
- ord-c76abc8690fc4a42adb75db60545b902
- Source dataset
- uspto-grants-2013_09
- Patent number
- US08535849B2
Linked notes
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