3,5-Dichloroaniline → N-(3,5-Dichlorophenyl)-2-hydroxy-1-naphthamide

HRID 421017

Reaction equation

HRID 421017 reaction equation
[OH:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]=1[C:12]([OH:14])=O.[Cl:15][C:16]1[CH:17]=[C:18]([CH:20]=[C:21]([Cl:23])[CH:22]=1)[NH2:19]>>[Cl:15][C:16]1[CH:17]=[C:18]([NH:19][C:12]([C:3]2[C:4]3[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=3)[CH:10]=[CH:11][C:2]=2[OH:1])=[O:14])[CH:20]=[C:21]([Cl:23])[CH:22]=1

Participants

3

Reactant 2

HCID 122813,5-DichloroanilineHCID 167902-Hydroxy-1-naphthoic acid

Product 1

HCID 11724295N-(3,5-Dichlorophenyl)-2-hydroxy-1-naphthamideYield 51.2%

Procedure

Using 2-hydroxynaphthalene-1-carboxylic acid and 3,5-dichloroaniline as the raw materials, the same operation as the example 16 gave the title compound.

Sources & evidence

ORD record
ord-d3a0ea052945469aab1c46aaddbaa0cd
Source dataset
uspto-grants-2012_01
Patent number
US08097759B2

Linked notes

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