Hydrochloric Acid → Citrulline

HRID 422898

Reaction equation

HRID 422898 reaction equation
Cl.[NH:2](C(OC(C)(C)C)=O)[C@H:3]([C:11]([OH:13])=[O:12])[CH2:4][CH2:5][CH2:6][NH:7][C:8]([NH2:10])=[O:9]>O1CCOCC1>[NH2:2][C@H:3]([C:11]([OH:13])=[O:12])[CH2:4][CH2:5][CH2:6][NH:7][C:8]([NH2:10])=[O:9]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 7021414Boc-Cit-OH

Product 1

HCID 9750Citrulline

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

10 mL of 4N HCl in dioxane were added to the 200 mg (0.200 g) Boc-Cit-Amp. The mixture was stirred at room temperature for 6 hours and solvent was removed.

Workup

  1. customsolvent was removed

Sources & evidence

ORD record
ord-06ce389f07cc4ad39e19449ddd941284
Source dataset
uspto-grants-2012_01
Patent number
US08101661B2

Linked notes

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