Sodium Iodide → 6-(4-Chlorophenyl)hexyl iodide

HRID 426873

Reaction equation

HRID 426873 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13]Br)=[CH:4][CH:3]=1.[I-:15].[Na+]>CC(C)=O>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][I:15])=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 5806791-(6-Bromohexyl)-4-chlorobenzene

Product 1

HCID 234557936-(4-Chlorophenyl)hexyl iodide

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

6-(4-Chlorophenyl)hexyl iodide [VIa; Ar is 4-ClC6H4, R is H] was prepared from 17 g. of 6-(4-chlorophenyl)hexyl bromide (Preparation C13) and 10.2 g. of sodium iodide in 325 ml. of acetone, to give 21 g. of product as an oil.

Sources & evidence

ORD record
ord-728be4e7078947ce9e184a806c6099a8
Source dataset
uspto-grants-1979_10
Patent number
US04171378

Linked notes

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