Cadmium chloride, dihydrate → 5-Chloro-2-methyl-3-isothiazolone cadmium(II)chloride
Reaction equation
[Cl-:1].[Cd+2:2].[Cl-].[Cl:4][C:5]1[S:9][N:8]([CH3:10])[C:7](=[O:11])[CH:6]=1>C(O)C>[Cl:4][C:5]1[S:9][N:8]([CH3:10])[C:7](=[O:11])[CH:6]=1.[Cl-:1].[Cd+2:2].[Cl-:4]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
To a solution of 5.5 g (0.03 mole) of anhydrous cadmium chloride in 120 ml of ethanol was added a solution of 4.5 g (0.03 mole) of 5-chloro-2-methyl-3-isothiazolone in 25 ml of ethanol. A white precipitate formed immediately. The mixture was filtered and air dried to yield 10.0 g (100%) of product, m.p. >250° C.
Workup
- customA white precipitate formed immediately
- filtrationThe mixture was filtered
- customair dried
Sources & evidence
- ORD record
- ord-241ae64773394f13b9e7dc796654469b
- Source dataset
- uspto-grants-1983_08
- Patent number
- US04396413
Reaction notes
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