HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → N,N'-Heptamethylenebis(4-pentyloxybenzamide)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 1,7-Heptanediamine | HCID 69533 | — |
| Reactant | p-Pentoxybenzoyl chloride | HCID 94910 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | N,N'-Heptamethylenebis(4-pentyloxybenzamide) | HCID 21453005 | — |
Reaction Steps
m.p. 155°-156° C., 29.9 g., was prepared as in Example 1 using 50 g. of 4-pentyloxybenzoyl chloride in 200 ml. of ethylene dichloride, 13.0 g. of 1,7-heptanediamine, 250 ml. of 10% aqueous potassium hydroxide solution, 500 ml. of ethylene dichloride and recrystallization from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009208 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-237b5978bc3f4f54b0c9a58e51765442 |
| Source note | uspto-grants-1977_02 |