HRID436636

反应详情

EQUATION

反应方程式

HRID 436636 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

m.p. 155°-156° C., 29.9 g., was prepared as in Example 1 using 50 g. of 4-pentyloxybenzoyl chloride in 200 ml. of ethylene dichloride, 13.0 g. of 1,7-heptanediamine, 250 ml. of 10% aqueous potassium hydroxide solution, 500 ml. of ethylene dichloride and recrystallization from ethanol.

WORKUP

后处理

  1. custom, was prepared as in Example 1 using 50 g
  2. customof ethylene dichloride and recrystallization from ethanol