2-Propenoic acid, 3-phenyl- → alpha-Hexylcinnamaldehyde
Reaction equation
[C:1]([OH:11])(=O)[CH:2]=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1>CC(O)COC(CO)C>[CH3:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]/[C:2](/[CH:1]=[O:11])=[CH:3]\[C:4]1[CH:5]=[CH:6][CH:7]=[CH:8][CH:9]=1Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
Solid at 10°-23° C. At higher temperature, yellowish, oily liquid which has a high tendency to oxidation (cinnamic acid). Dissolves readily in diethyl phthalates and dipropylene glycol, floral, fruity note.
Workup
- customat 10°-23° C
Sources & evidence
- ORD record
- ord-e0221868185840c6abfc562742b544b1
- Source dataset
- uspto-grants-1996_05
- Patent number
- US05518997
Reaction notes
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