Salicylaldehyde → HCID 69497707, compound

HRID 460662

Reaction equation

HRID 460662 reaction equation
[CH:1](=O)[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[C:10]1(=[O:16])[O:15][CH:13]([CH3:14])[CH2:12][CH2:11]1>C1(C)C=CC=CC=1>[OH:4][C:3]1[CH:5]=[CH:6][CH:7]=[CH:8][C:2]=1[CH:1]=[C:11]1[CH2:12][CH:13]([CH3:14])[O:15][C:10]1=[O:16]

Participants

4

Reactant 2

HCID 6998SalicylaldehydeHCID 7921Gamma-Valerolactone

Product 1

HCID 69497707HCID 69497707, compoundYield 66.9%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Salicylaldehyde (15.2 g) and γ-valerolactone (25 g) were dissolved in toluene (150 ml). By the reactions as in the same manner as in Example 307, the title compound (17 g) was obtained, melting point 112–114° C.

Sources & evidence

ORD record
ord-b7558b236a9d4731b3ff9f454b289deb
Source dataset
uspto-grants-2007_03
Patent number
US07196199B2

Linked notes

Loading…