2-Ethylhexylamine → HCID 178438302, compound

HRID 462561

Reaction equation

HRID 462561 reaction equation
[CH2:1]([C:4]12[CH2:10][CH:7]([CH:8]=[CH:9]1)[CH:6]1[C:11]([O:13][C:14](=[O:15])[CH:5]21)=[O:12])[CH:2]=[CH2:3].[CH2:16]([CH:18]([CH2:21][CH2:22][CH2:23][CH3:24])[CH2:19][NH2:20])[CH3:17]>>[CH2:16]([CH:18]([CH2:21][CH2:22][CH2:23][CH3:24])[CH2:19][N:20]=[C:14]([CH:5]1[CH:6]([C:11]([OH:13])=[O:12])[CH:7]2[CH2:10][C:4]1([CH2:1][CH:2]=[CH2:3])[CH:9]=[CH:8]2)[OH:15])[CH3:17]

Participants

3

Reactant 2

HCID 77192-EthylhexylamineHCID 54206110HCID 54206110, compound

Product 1

HCID 178438302HCID 178438302, compound

Procedure

The procedure described in Example 3 is repeated, except that 204 g of allyl-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid anhydride and 129 g of 2-ethylhexylamine are used. 17 g of water are split off at 115° to 160° C. under 4,000 Pa in the course of 4.5 hours. 292.05 g (92.6% of theory) of a fraction of boiling point 160°-164° C. under 10.7 Pa, nD20 1.5038 and η25 0.68 Pa.s are obtained.

Workup

  1. custom17 g of water are split off at 115° to 160° C. under 4,000 Pa in the course of 4.5 hours
  2. custom292.05 g (92.6% of theory) of a fraction of boiling point 160°-164° C. under 10.7 Pa, nD20 1.5038 and η25 0.68 Pa.s are obtained

Sources & evidence

ORD record
ord-66646a12f77d4dda98649accf3d14af1
Source dataset
uspto-grants-1985_05
Patent number
US04515962

Linked notes

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