HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 3-Phenyl-1-indanone oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Indanone, 3-phenyl- | HCID 98146 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-Phenyl-1-indanone oxime | HCID 73183939 | — |
Reaction Steps
A mixture of 3-phenylindan-1-one (80 g), methanol (935 ml), water (90 ml), potassium carbonate (103.8 g), and hydroxylamine HCl (104.3 g) was heated at reflux for 16 hours, then poured into ice-water: the title compound was filtered, washed with water, with a small portion of ether, then dried in air. Yield: 74.7 g; m.p. 133°-139°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04548946 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-06804961a4a94f6fab538831a07fec43 |
| Source note | uspto-grants-1985_10 |