反应详情

A mixture of 3-phenylindan-1-one (80 g), methanol (935 ml), water (90 ml), potassium carbonate (103.8 g), and hydroxylamine HCl (104.3 g) was heated at reflux for 16 hours, then poured into ice-water: the title compound was filtered, washed with water, with a small portion of ether, then dried in air. Yield: 74.7 g; m.p. 133°-139°.

1. temperaturewas heated
2. temperatureat reflux for 16 hours
3. filtrationthe title compound was filtered
4. washwashed with water, with a small portion of ether
5. customdried in air