Hydrochloric Acid → HCID 178421680, compound
Reaction equation
C(N[C:6](=[O:13])[C:7]([C:9]1([CH3:12])[CH2:11][CH2:10]1)=O)(C)(C)C.[NH2:14][NH:15][C:16]([NH:18][NH2:19])=[S:17].Cl.C(O)C>O>[NH2:14][N:15]1[C:6](=[O:13])[C:7]([C:9]2([CH3:12])[CH2:11][CH2:10]2)=[N:19][N:18]=[C:16]1[SH:17]Participants
6
Reactant 4
Product 1
Reagents, catalysts & solvents 1
Procedure
183 grams of (1-methyl-cyclopropyl)-glyoxalic acid-tert.-butylamide and 112 grams of thiocarbohydrazide were added to a mixture of 1 liter of 1 normal HCl and 1 liter of ethanol. The mixture was boiled under reflux for 8 hours, cooled, diluted with 2 liters of water and the crystals filtered off with suction. There were obtained white crystals with a yellow luster which were dried.
Workup
- temperatureunder reflux for 8 hours
- temperaturecooled
- filtrationthe crystals filtered off with suction
- customThere were obtained white crystals with a yellow luster which
- customwere dried
Sources & evidence
- ORD record
- ord-e471648b4ae44be4b25f0eae45b4618f
- Source dataset
- uspto-grants-1979_11
- Patent number
- US04175188
Reaction notes
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