Ethyl 2-chloroacetoacetate → HCID 86633755, compound

HRID 475558

Reaction equation

HRID 475558 reaction equation
Cl[CH:2]([C:8]([CH3:10])=O)[C:3]([O:5][CH2:6][CH3:7])=[O:4].[CH2:11]([O:13][C:14]1[CH:15]=[C:16]([CH:20]=[CH:21][C:22]=1[O:23][CH2:24]C)[C:17]([NH2:19])=[O:18])C>>[CH3:11][O:13][C:14]1[CH:15]=[C:16]([C:17]2[O:18][CH:10]=[C:8]([CH2:2][C:3]([O:5][CH2:6][CH3:7])=[O:4])[N:19]=2)[CH:20]=[CH:21][C:22]=1[O:23][CH3:24]

Participants

3

Reactant 2

HCID 11858Ethyl 2-chloroacetoacetateHCID 3403423,4-Diethoxybenzamide

Product 1

HCID 86633755HCID 86633755, compound

Procedure

Using ethyl 2-chloroacetoacetate and 16 g of 3,4-diethoxybenzamide and following the procedure of Reference Example 5, 3.8 g of ethyl [2-(3,4-dimethoxyphenyl)oxazol-4-yl]acetate was obtained.

Sources & evidence

ORD record
ord-e67960cef2ea42b7b4b36219bd4de4c1
Source dataset
uspto-grants-2014_01
Patent number
US08637559B2

Linked notes

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