Sodium Carbonate → HCID 14234820, compound
Reaction equation
Cl.[NH2:2][CH:3]1[CH2:15][C:14]2[C:6](=[CH:7][C:8]3[CH2:12][CH2:11][O:10][C:9]=3[CH:13]=2)[CH2:5][CH2:4]1.[CH2:16]([O:18][CH2:19][CH2:20]Br)[CH3:17].C(=O)([O-])[O-].[Na+].[Na+]>C(O)C>[CH2:16]([O:18][CH2:19][CH2:20][NH:2][CH:3]1[CH2:15][C:14]2[C:6](=[CH:7][C:8]3[CH2:12][CH2:11][O:10][C:9]=3[CH:13]=2)[CH2:5][CH2:4]1)[CH3:17]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
A mixture containing 7.8 g of the compound of Example 2, 6.7 g of 2-bromoethyl ethyl ether and 6.2 g of sodium carbonate in ethanol is brought to reflux with stirring for 20 hours.
Workup
- temperatureto reflux
Sources & evidence
- ORD record
- ord-4bcdb6f992fb4207a2c78dc5b16c6de6
- Source dataset
- uspto-grants-1989_12
- Patent number
- US04885373
Reaction notes
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