Hydroxyamine hydrochloride → HCID 18001652, compound

Reaction equation

[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][N:8]2[CH2:13][CH2:12][C:11](=O)[CH2:10][CH2:9]2)[CH:2]=1.Cl.[NH2:16][OH:17]>>[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][N:8]2[CH2:13][CH2:12][C:11](=[N:16][OH:17])[CH2:10][CH2:9]2)[CH:2]=1

Participants

Reactant 2

HCID 443297Hydroxyamine hydrochloride

HCID 64216241-(Pyridin-3-ylmethyl)piperidin-4-one

Product 1

HCID 18001652HCID 18001652, compound

Procedure

1-(3-Pyridinylmethyl)-4-piperidone oxime is prepared from 1-(3-pyridinylmethyl)-4-piperidone and hydroxylamine hydrochloride essentially as described above in Example 38, Scheme C, step b.

Sources & evidence

ORD record: ord-23ee7ce6356e41aeadd490a581c35f4f
Source dataset: uspto-grants-2003_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06642231B2

Reaction notes

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