Ethylenediamine → N-Cyclohexyl-1,2-ethanediamine

HRID 483682

Reaction equation

HRID 483682 reaction equation
[CH2:1]([NH2:4])[CH2:2][NH2:3].[C:5]1(=O)[CH2:10][CH2:9][CH2:8][CH2:7][CH2:6]1>[Pt]>[CH:5]1([NH:3][CH2:2][CH2:1][NH2:4])[CH2:10][CH2:9][CH2:8][CH2:7][CH2:6]1

Participants

4

Reactant 2

HCID 3301EthylenediamineHCID 7967Cyclohexanone

Product 1

HCID 21922N-Cyclohexyl-1,2-ethanediamine

Reagents, catalysts & solvents 1

HCID 23939PlatinumCatalyst

Procedure

In this example the ratio of ethylenediamine:cyclohexanone, the reaction temperature, and the H2 :feed ratio were varied using as a catalyst 0.3 weight percent platinum (sulfided) on gamma-alumina in a non-aqueous environment. Samples were taken every 6 hours to afford the results in Table 1.

Workup

  1. customto afford the
  2. customresults in Table 1

Sources & evidence

ORD record
ord-e22953cfec3f4539836cce62709883d5
Source dataset
uspto-grants-1993_07
Patent number
US05225597

Linked notes

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