Homoveratrylamine → 3-((2-(3,4-Dimethoxyphenyl)ethyl)amino)butyronitrile
Reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:11][CH2:12][NH2:13])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10].[C:14](#[N:18])/[CH:15]=[CH:16]/[CH3:17]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:11][CH2:12][NH:13][CH:16]([CH3:17])[CH2:15][C:14]#[N:18])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10]Participants
3
Conditions
- Temperature
- 100 °C
Procedure
A mixture of 10.0 g of 2-(3,4-dimethoxyphenyl)ethylamine with 14 ml of crotononitrile was stirred at 100° C. for 30 h.
Sources & evidence
- ORD record
- ord-3f8a0cf7a32a4dd08d2e8e75ad0f91ab
- Source dataset
- uspto-grants-1994_03
- Patent number
- US05292770
Reaction notes
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