HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 19091770, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Diethyl iminodiacetate | HCID 80502 | — |
| Reactant | 3,5-Bis[(11-methoxy-11-oxoundecyl)oxy]benzoic acid | HCID 19091815 | — |
| Product | HCID 19091770 | HCID 19091770 | — |
Reaction Steps
Conversion of 3,5-bis[(11-methoxy-11-oxoundecyl)oxy]benzoic acid to the acid chloride with thionyl chloride followed by treatment with diethyl iminodiacetate as in Example 21 gave N-(2-ethoxy-2-oxoethyl)-N-[3,5-bis[(11-methoxy-11-oxoundecyl)oxy]-benzoyl]glycine ethyl ester as an oil after chromatography on 125 g of silica gel using 20% ethyl acetate-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05298652 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-4bce587ed8fb44b799c628fdff238b49 |
| Source note | uspto-grants-1994_03 |