HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 488982Generated: October 25, 2026
Aluminum sec-butoxide → 2,9-Dihexylpentacene
https://huagongshe.com/reaction/488982
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Aluminum sec-butoxide | HCID 61289 | — |
| Reactant | 3,10-Dihexylpentacene-5,12-dione | HCID 22269484 | — |
| Solvent | Mesitylene | HCID 7947 | — |
| Product | 2,9-Dihexylpentacene | HCID 17973372 | — |
Reaction Steps
A mixture of 1.0 grams of 3,10-dihexylpentacene-5,12-dione and 2.5 grams of aluminum tri(sec-butoxide) in 50 mL of mesitylene was heated to 155° C. for 2 days and cooled. The reaction mixture was filtered and the residue washed with concentrated HCl to give 2,9-dihexylpentacene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06974877B2 |
|---|
| Source dataset | uspto-grants-2005_12 |
|---|
| ORD ID | ord-2c8db88bb45447ab8ec829bde259eb2e |
|---|
| Source note | uspto-grants-2005_12 |
|---|
