Ammonia → HCID 178512765, compound

HRID 49934

Reaction equation

HRID 49934 reaction equation
[NH2:1][CH2:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=[O:8])=[CH:5][CH:4]=1.N.[N:13]#[C:14][NH2:15]>O>[NH:1]([CH2:2][C:3]1[CH:4]=[CH:5][C:6]([C:7]([OH:9])=[O:8])=[CH:10][CH:11]=1)[C:14]([NH2:15])=[NH:13]

Participants

5

Reactant 3

HCID 222AmmoniaHCID 9864CyanamideHCID 655264-(Aminomethyl)Benzoic Acid

Product 1

HCID 178512765HCID 178512765, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
60 °C

Procedure

A mixture of 1.51 g (10.0 mmol) of 4-aminomethylbenzoic acid, 20 ml of water, 2.0 ml of 28% aqueous ammonia and 1.00 g (23.8 mmol) of cyanamide was stirred at 60° C. overnight. The white precipitate thus formed was taken by the filtration, washed with water and dried to obtain the title compound.

Workup

  1. customThe white precipitate thus formed
  2. filtrationwas taken by the filtration
  3. washwashed with water
  4. customdried

Sources & evidence

ORD record
ord-c887df8de4df4a55a09c1569fe4de64f
Source dataset
uspto-grants-2004_03
Patent number
US06710056B2

Linked notes

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