Dodecane → Quinoline

HRID 52792

Reaction equation

[NH2:1]C1C(I)=C(C(O)=O)C(I)=C(C(O)=O)C=1I.CCC[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28]>>[N:1]1[C:20]2[C:25](=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:26]=[CH:27][CH:28]=1

Participants

Reactant 2

HCID 8182Dodecane

HCID 30157835-Amino-2,4,6-triiodo-1,3-benzenedicarboxylic acid

Product 1

HCID 7047QuinolineYield 95.6%

Procedure

According to the procedure described in Example 1, the reaction is carried out with the same amounts of 5-amino-2,4,6-triiodo-1,3-benzenedicarboxylic acid using n-dodecane instead of meta-xylene, with quinoline, giving a yield of 95.6%.

Sources & evidence

ORD record: ord-9c6766f2e63c45fd87dad080214aa048
Source dataset: uspto-grants-1997_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05616795

Linked notes

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