Hydrochloric Acid → HCID 15578422, compound
Reaction equation
[C:1]1([C:11](=[O:23])[CH2:12][C:13](=[O:22])[CH2:14][C:15](=O)[C:16]([O:18]CC)=[O:17])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.Cl>O1CCOCC1>[C:1]1([C:11]2[O:23][C:15]([C:16]([OH:18])=[O:17])=[CH:14][C:13](=[O:22])[CH:12]=2)[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
This crude ester was dissolved in dioxan (50 ml) and concentrated hydrochloric acid (50 ml), and the solution was heated under reflux for 11/2 hours then concentrated under vacuum to give a brown solid. The solid was recrystallised from ethanol and from ethanol-water to give the title product (mp 248°-249° C. with decomposition).
Workup
- temperature